J-HMBC and XLOC for Varian

Download package:

gjhmbc.tar.Z

Content of package

Pulse Program: gj_hmbc.c
VNMR Macros: JHMBC Macro for parameter setup
XLOC Macro for parameter setup
bbhmbc_proc Processing routine for automatic processing and dataset combination in absolute-value mode
C-Routines: ed_sort.c Routine for sorting edited subspectra
av_add.c Routine for adding processed data in absolute-value mode
Shell Scripts: bb_hmbc Shell script used by bbhmbc_proc macro for editing and sorting of raw data
gjhmbc_install Script for installation and compilation of J-HMBC / XLOC package components
Parameter files: GJ_HMBC.par/procpar J-HMBC parameter
GJ_HMBC.par/text pp identifier

Programs tested on:

Varian Unity Inova, Vnmr 6.1B, Pbox 6.1C, Solaris 7

Installation:

For installation the compressed archive gjhmbc.tar.Z containing the source codes of all components is required. The installation can either be executed for individual users or globally for all users within the vnmr1 account.

Content of installation package: gjhmbc_v1.tar.Z, gjhmbc_install, GJHMBC_README

  1. Login at the user account in which the installation should be carried out
  2. Save the gjhmbc.tar.Z file at a location with write permission for the user who is carrying out the installation.
  3. Unpack the file with the commands: uncompress gjhmbc.tar.Z and tar -xvf gjhmbc.tar
  4. Run the gjhmbc_install script, answer all questions. (Installation for vnmr1 can be executed either as local installation for vnmr1 only or as global installation for all users)
  5. Installation is completed successfully when the installation script runs without any error. The installation files can be removed after successful installation.

    Performing Experiments:

    To set up an experiment the JHMBC or XLOC macro can be used.
    1. Run a 1D spectrum and adjust sw, pw, np,
    2. Call the JHMBC or XLOC macro to generate the corresponding dataset.
    3. Adjust 2D parameters if necessary. Default values are
      • sw1 = 205 ppm -> -5 ppm
      • delays for long-range evolution (Four Values: 440.7, 343.4, 290.3, 242.2 ms)
      • ni = 256
      • nt = 4.
    4. Adjust the receiver gain and start the experiment (go)
    5. For processing J-HMBC spectra use the wft2da command, for Broadband XLOC run the bbhmbc_proc macro and answer all questions (make sure all gjhmbc components are installed the right way). This will perform the complete processing, and broadband combination automatically
 
Document: J-HMBC and XLOC for Varian (index.shtml)
Last modified: 2005-12-19